Data quality metrics extracted from 1ztf.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1ZTF at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 22-ID
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
22-ID
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2004-07-06
Detector
_diffrn_detector.type
MARRESEARCH
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9794, 0.9795, 1.0000
Software
Data collection
_software.classification
MAR345
Data scaling
_software.classification
HKL-2000
Phasing
_software.classification
SHARP
Refinement
_software.classification
REFMAC (5.2.0005)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 1 21 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
42.987 52.701 63.779 90.00 108.89 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979400.979501.00000 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 40.000
High resolution limit [Å] 
_reflns.d_resolution_high
 1.990
Rmerge 
_reflns.pdbx_Rsym_value
 0.066
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 18215
  <I/σ(I)> -
  Completeness [%] -
Multiplicity 
_reflns.pdbx_redundancy
 3.7
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1ZTF
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-05-26
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
39.8 - 1.990 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1630 / 0.2357
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD