Data quality metrics extracted from 1zs9.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1ZS9 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
BSRF BEAMLINE 3W1A
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
BSRF
Beamline
_diffrn_source.pdbx_synchrotron_beamline
3W1A
Temperature [K]
_diffrn.ambient_temp
100.0
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2003-10-09
Detector
_diffrn_detector.type
MARRESEARCH
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9000, 0.9798, 0.9800
Software
Data collection
_software.classification
AUTOMAR
Data reduction
_software.classification
AUTOMAR
Phasing
_software.classification
SOLVE
Refinement
_software.classification
CNS (1.0)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
54.017 57.546 87.318 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.900000.979800.98000 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 30.000 1.770
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 1.700 1.700
  Rmerge - -
  Rmeas - -
  Rpim - -
  Total number of observations - -
  Total number unique - -
  <I/σ(I)> - -
  Completeness [%] - -
  Multiplicity - -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1ZS9
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-05-23
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
30.0 - 1.700 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2080 / 0.2410
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD