| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | NSLS BEAMLINE X25 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | NSLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X25 |
Temperature [K] _diffrn.ambient_temp | 80 |
Detector technology _diffrn_detector.detector | PIXEL |
Collection date _diffrn_detector.pdbx_collection_date | 2013-04-16 |
Detector _diffrn_detector.type | PSI PILATUS 6M |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 1.1 |
| Software | |
Data reduction _software.classification | HKL-2000 (2.3.2) |
Data scaling _software.classification | HKL-2000 (2.3.2) |
Phasing _software.classification | PHENIX (1.8.2) |
Model building _software.classification | Coot (Coot 0.7) |
Refinement _software.classification | PHENIX (dev_2006) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 77.906 61.759 85.336 90.0 116.2 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.10000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 76.570 |
High resolution limit [Å] _reflns.d_resolution_high | 1.620 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.153 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 87993 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 34.58 |
Completeness [%] _reflns.percent_possible_obs | 95.0 |
Multiplicity _reflns.pdbx_redundancy | 5.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 4ZC4 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2015-04-15 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 38.3 - 1.860 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1815 / 0.2137 |
Structure solution method _refine.pdbx_method_to_determine_struct | MAD |