Data quality metrics extracted from 1zbb.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1ZBB at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SLS BEAMLINE X06SA
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SLS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
X06SA
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2003-10-03
Detector
_diffrn_detector.type
MARRESEARCH
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.850030
Software
Phasing
_software.classification
BEAST
Model building
_software.classification
BEAST
Refinement
_software.classification
REFMAC (5.1.24)
General information
Spacegroup name
_symmetry.space_group_name_H-M
I 2 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
127.675 168.445 237.126 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.969801.000030.85003 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 50.000 10.000
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 9.000 9.000
Rmerge 
_reflns.pdbx_Rsym_value _reflns_shell.pdbx_Rsym_value
 0.072 0.087
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 1994 542
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 17.28 12.55
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 97.0 97.4
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 5.7 4.2
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1ZBB
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2005-04-08
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
50.0 - 9.000 Å
R
_refine.ls_R_factor_obs
0.3860
Rwork
_refine.ls_R_factor_R_work
0.3860
WARNING: no Rfree given?
Structure solution method
_refine.pdbx_method_to_determine_struct
MOLECULAR REPLACEMENT
Starting model (for MR)
_refine.pdbx_starting_model
1KX5(NUCLEOSOME CORE PARTICLE)