Data quality metrics extracted from 2yz4.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2YZ4 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
NEUTRON DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
LAUE
Temperature [K]
_diffrn.ambient_temp
293
Detector technology
_diffrn_detector.detector
LADI
Collection date
_diffrn_detector.pdbx_collection_date
2005-06-01
Detector
_diffrn_detector.type
IMAGE PLATE
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
2.9-3.9
Software
Data collection
_software.classification
LADI (SPEC)
Data reduction #1
_software.classification
LAUEGEN
Data reduction #2
_software.classification
LSCALE
Data scaling
_software.classification
SCALA (Phil Evans; pre@mrc-lmb.cam.ac.uk)
Phasing
_software.classification
CNS (1.1)
Refinement
_software.classification
CNS (1.1; Axel T. Brunger; axel.brunger@yale.edu)
General information
Spacegroup name
_symmetry.space_group_name_H-M
I 2 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
89.377 87.314 63.051 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
2.900003.90000 Å

Data quality metricsOverallInnerShellOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 33.653 33.650 2.320
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.181 6.960 2.200
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.213 0.114 0.314
  Rmeas - - -
  Rpim - - -
Total number of observations 
_reflns_shell.number_measured_all
 - 2147 3484
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 8512 416 861
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 2.80 4.50 1.90
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 67.2 94.3 46.9
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 6.2 5.2 4.0
  CC(1/2) - - -

Refinement
PDB entry ID
_entry.id
2YZ4
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2007-05-02
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
33.6 - 2.200 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2790 / 0.3120
Structure solution method
_refine.pdbx_method_to_determine_struct
MOLECULAR REPLACEMENT
Starting model (for MR)
_refine.pdbx_starting_model
PDB ENTRY 1NLS