| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SPRING-8 BEAMLINE BL44B2 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SPring-8 |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL44B2 |
Collection date _diffrn_detector.pdbx_collection_date | 2004-11-15 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.7000 |
| Software | |
Phasing _software.classification | SHELX |
Model building _software.classification | SHELX |
Refinement _software.classification | SHELXL-97 |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 51.936 67.592 34.588 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.70000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 20.600 |
High resolution limit [Å] _reflns.d_resolution_high | 1.000 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 65863 |
| <I/σ(I)> | - |
| Completeness [%] | - |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2YYX |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2007-05-02 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 1.000 Å |
Structure solution method _refine.pdbx_method_to_determine_struct | AB INITIO |