Data quality metrics extracted from 2yvx.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2YVX at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SPRING-8 BEAMLINE BL41XU
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SPring-8
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL41XU
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2006-11-28
Detector
_diffrn_detector.type
ADSC QUANTUM 315
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97924, 0.97933, 0.98200
Software
Data collection
_software.classification
ADSC (Quantum)
Data reduction
_software.classification
DENZO
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
SHARP
Refinement
_software.classification
CNS (1.2)
General information
Spacegroup name
_symmetry.space_group_name_H-M
C 2 2 21
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
118.314 134.897 366.252 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979240.979330.98200 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 50.000 3.560
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 3.500 3.500
Rmerge 
_reflns.pdbx_Rsym_value _reflns_shell.pdbx_Rsym_value
 0.110 0.453
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 37118 -
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 8.60 2.30
  Completeness [%] - -
Multiplicity 
_reflns.pdbx_redundancy
 16.0 -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
2YVX
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2007-04-18
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
49.7 - 3.500 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2940 / 0.3410
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD