| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | PHOTON FACTORY |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Photon Factory |
Temperature [K] _diffrn.ambient_temp | 278.00 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1988-01-01 |
Detector _diffrn_detector.type | Y.AMEMIYA |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling _software.classification | SCALEPACK |
Phasing #1 _software.classification | MLPHARE |
Phasing #2 _software.classification | DM |
Model building #1 _software.classification | PHARE |
Model building #2 _software.classification | DENMOD |
Refinement #1 _software.classification | NUCLIN/PROFFT |
Refinement #2 _software.classification | MODIFIED (BY Z.OTWINOWSKI) |
Refinement #3 _software.classification | NUCLIN |
Refinement #4 _software.classification | PROFFT (MODIFIED BY Z.OTWINOWSKI) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 64 2 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 113.720 113.720 136.541 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 20.000 |
High resolution limit [Å] _reflns.d_resolution_high | 3.000 |
Rmerge _reflns.pdbx_Rsym_value | 0.080 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 10688 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 15.70 |
Completeness [%] _reflns.percent_possible_obs | 95.0 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1YFG |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-05-08 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 3.000 Å |
Structure solution method _refine.pdbx_method_to_determine_struct | MIR |
Starting model _refine.pdbx_starting_model | 4 A STRUCTURE REPORTED IN REFERENCE 2 |