Data quality metrics extracted from 1y8a.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1Y8A at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 19-BM
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
19-BM
Temperature [K]
_diffrn.ambient_temp
110
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2004-04-18
Detector
_diffrn_detector.type
CUSTOM-MADE
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97951
Software
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
SCALEPACK
Phasing #1
_software.classification
SHELXD
Phasing #2
_software.classification
MLPHARE
Phasing #3
_software.classification
autoSHARP
Refinement
_software.classification
REFMAC (5.2.0005)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
74.900 84.027 44.175 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979440.97951 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 36.640 1.450
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 1.400 1.400
  Rmerge - -
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 53385 -
  <I/σ(I)> - -
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 96.0 70.2
  Multiplicity - -
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1Y8A
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2004-12-10
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
36.6 - 1.400 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1828 / 0.2227
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD