| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | EMBL/DESY, HAMBURG BEAMLINE X31 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | EMBL/DESY, HAMBURG |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X31 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1993-08-18 |
Detector _diffrn_detector.type | CUSTOM-MADE |
| Software | |
Data reduction _software.classification | MOSFLM |
Phasing _software.classification | X-PLOR |
Model building _software.classification | X-PLOR |
Refinement #1 _software.classification | SHELXL-93 |
Refinement #2 _software.classification | PROLSQ |
Refinement #3 _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 73.45 68.94 58.76 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.92000 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1XSO |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-03-14 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 1.490 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1040 / 0.1690 |