| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | EMBL/DESY, HAMBURG |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BW7B |
Collection date _diffrn_detector.pdbx_collection_date | 1995-11-25 |
Detector _diffrn_detector.type | MARRESEARCH |
| Software | |
Data reduction _software.classification | DENZO |
Data scaling _software.classification | SCALEPACK |
Phasing _software.classification | X-PLOR |
Model building _software.classification | X-PLOR |
Refinement #1 _software.classification | PROLSQ |
Refinement #2 _software.classification | REFMAC |
Refinement #3 _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 31 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 81.26 81.26 72.60 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.85900 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1WAB |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-10-30 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 8.5 - 1.700 Å |
Rwork _refine.ls_R_factor_R_work | 0.1954 WARNING: no Rfree given (but Rwork)!? |