Data quality metrics extracted from 2w8m.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2W8M at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SSRL BEAMLINE BL9-1
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SSRL
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BL9-1
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2008-01-21
Detector
_diffrn_detector.type
ADSC CCD
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.77, 0.98
Software
Data reduction
_software.classification
DENZO
Data scaling
_software.classification
SCALEPACK
Phasing #1
_software.classification
SOLVE
Phasing #2
_software.classification
RESOLVE
Refinement
_software.classification
REFMAC (5.2.0019)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 1 21 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
56.477 81.971 60.160 90.0 115.4 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.850002.060000.770000.98000 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 30.000 2.490
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.400 2.400
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.030 0.330
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs
 17143 -
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 32.00 4.30
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 92.9 95.7
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 3.1 3.0
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
2W8M
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2009-01-17
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
29.1 - 2.400 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2090 / 0.2450
Structure solution method
_refine.pdbx_method_to_determine_struct
MIRAS
Starting model
_refine.pdbx_starting_model
NONE