Data quality metrics extracted from 3vxf.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 3VXF at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Method
_exptl.method
NEUTRON DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
NUCLEAR REACTOR
Source details
_diffrn_source.type
JRR-3M BEAMLINE 1G-C
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
JRR-3M
Beamline
_diffrn_source.pdbx_synchrotron_beamline
1G-C
Temperature [K]
_diffrn.ambient_temp
298
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
2009-03-23
Detector
_diffrn_detector.type
BIX-4
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
2.6
Software
Data reduction
_software.classification
DENZO
Data scaling
_software.classification
SCALEPACK
Refinement
_software.classification
PHENIX (PHENIX.REFINE: DEV_663)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
80.998 107.800 45.888 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.000002.60000 Å

Data quality metricsOverallInnerShellOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 50.000 50.000 1.660
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 1.600 3.450 1.600
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.051 0.036 0.332
  Rmeas - - -
  Rpim - - -
  Total number of observations - - -
Total number unique 
_reflns.number_obs
 51182 - -
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 34.50 45.60 5.20
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 95.6 75.3 97.1
  Multiplicity - - -
  CC(1/2) - - -

Refinement
PDB entry ID
_entry.id
3VXF
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2012-09-12
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
44.9 - 2.752 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1828 / 0.2339