| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Temperature [K] _diffrn.ambient_temp | 277 |
Detector technology _diffrn_detector.detector | AREA DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 1986-08-05 |
Detector _diffrn_detector.type | XENTRONICS |
| Software | |
Data collection _software.classification | BUDDHA |
Data reduction #1 _software.classification | ROTAVATA |
Data reduction #2 _software.classification | Agrovata |
Data reduction #3 _software.classification | BUDDHA |
Data scaling #1 _software.classification | CCP4 (AGROVATA |
Data scaling #2 _software.classification | ROTAVATA |
Model building _software.classification | BRICOGNE |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 55.1 98.8 172.9 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 10.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.700 |
Rmerge _reflns.pdbx_Rsym_value | 0.102 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 24682 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 93.0 |
Multiplicity _reflns.pdbx_redundancy | 4.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2VSG |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-11-19 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 6.0 - 2.700 Å |
Rwork _refine.ls_R_factor_R_work | 0.2030 WARNING: no Rfree given (but Rwork)!? |
Structure solution method _refine.pdbx_method_to_determine_struct | SIRAS |