Data quality metrics extracted from 1vp7.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1VP7 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
ALS BEAMLINE 8.3.1
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
ALS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
8.3.1
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2004-09-18
Detector
_diffrn_detector.type
ADSC
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.979694,0.979811,1.020035
Software
Data reduction
_software.classification
MOSFLM
Data scaling #1
_software.classification
SCALA (5.0))
Data scaling #2
_software.classification
CCP4 (SCALA)
Phasing #1
_software.classification
autoSHARP
Phasing #2
_software.classification
SHELX
Model building
_software.classification
SHELX
Refinement
_software.classification
REFMAC (5.2.0005)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 6 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
107.03 107.03 207.26 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979690.979811.02004 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 29.020 2.530
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.400 2.400
Rmerge 
_reflns.pdbx_Rsym_value _reflns_shell.pdbx_Rsym_value
 0.130 0.616
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 28264 4033
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 18.00 3.60
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 99.9 100.0
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 11.7 6.8
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
1VP7
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2004-10-14
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
29.0 - 2.400 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2027 / 0.2444
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD