| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | ALS BEAMLINE 8.2.2 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | ALS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | 8.2.2 |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | AREA DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 2014-10-14 |
Detector _diffrn_detector.type | ADSC QUANTUM 315r |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.97965 |
| Software | |
Data reduction _software.classification | xia2 |
Data scaling _software.classification | xia2 |
Phasing _software.classification | AutoSol |
Refinement _software.classification | PHENIX (dev_2650: ???) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 54.79 74.06 81.36 116.80 105.19 90.78 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.97965 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 65.290 |
High resolution limit [Å] _reflns.d_resolution_high | 2.160 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 55872 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 8.50 |
Completeness [%] _reflns.percent_possible_obs | 95.7 |
Multiplicity _reflns.pdbx_redundancy | 3.2 |
CC(1/2) _reflns.pdbx_CC_half | 0.995 |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 5VL9 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2017-04-25 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 65.3 - 2.160 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1940 / 0.2288 |
Structure solution method _refine.pdbx_method_to_determine_struct | SAD |