Data quality metrics extracted from 8vjv.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 8VJV at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 24-ID-E
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
24-ID-E
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
PIXEL
Collection date
_diffrn_detector.pdbx_collection_date
2020-06-29
Detector
_diffrn_detector.type
DECTRIS EIGER X 16M
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.97912
Software
Data reduction
_software.classification
XDS
Data scaling
_software.classification
STARANISO
Phasing
_software.classification
PHASER
Refinement
_software.classification
PHENIX (1.20.1_4487)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 21 21 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
143.168 60.116 95.734 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.97912 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 95.734 2.244
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 2.120 2.123
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.138 2.326
Rmeas 
_reflns.pdbx_Rrim_I_all _reflns_shell.pdbx_Rrim_I_all
 0.146 2.462
Rpim 
_reflns.pdbx_Rpim_I_all _reflns_shell.pdbx_Rpim_I_all
 0.047 0.798
Total number of observations 
_reflns_shell.number_measured_all
 - 19296
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_obs
 42142 2090
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.pdbx_netI_over_sigmaI_obs
 10.30 1.40
Completeness [%] 
_reflns.percent_possible_obs
 88.7 -
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 9.5 9.2
  CC(1/2) - -

Refinement
PDB entry ID
_entry.id
8VJV
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2024-01-08
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
95.7 - 2.120 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2131 / 0.2492
Structure solution method
_refine.pdbx_method_to_determine_struct
MOLECULAR REPLACEMENT
Starting model (for MR)
_refine.pdbx_starting_model
WARNING: no starting model (for MR) given