| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | LAUE |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | ESRF BEAMLINE ID09 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | ESRF |
Beamline _diffrn_source.pdbx_synchrotron_beamline | ID09 |
Temperature [K] _diffrn.ambient_temp | 288.0 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2005-10-15 |
Detector _diffrn_detector.type | MAR CCD 130 mm |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.77-1.24 |
| Software | |
Data reduction #1 _software.classification | XFIT |
Data reduction #2 _software.classification | LaueView |
Data scaling _software.classification | LaueView |
Refinement _software.classification | SHELXL-97 |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 63 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 66.833 66.833 40.947 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.770001.24000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 28.900 |
High resolution limit [Å] _reflns.d_resolution_high | 1.600 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 13891 |
| <I/σ(I)> | - |
| Completeness [%] | - |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 3VE4 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2012-01-07 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 28.9 - 1.600 Å |
R _refine.ls_R_factor_obs | 0.2140 WARNING: no Rwork given |
Rfree _refine.ls_R_factor_R_free | 0.2520 |