| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | ROTATING ANODE |
Temperature [K] _diffrn.ambient_temp | 298 |
Detector technology _diffrn_detector.detector | AREA DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 1999-11-22 |
Detector _diffrn_detector.type | ENRAF-NONIUS |
| Software | |
Data reduction #1 _software.classification | MADNESS |
Data reduction #2 _software.classification | PROCOR |
Data scaling #1 _software.classification | Agrovata |
Data scaling #2 _software.classification | ROTAVATA |
Data scaling #3 _software.classification | SCALA |
Data scaling #4 _software.classification | TRUNCATE |
Phasing _software.classification | X-PLOR |
Refinement _software.classification | CNS (1.2) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | I 21 3 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 132.87 132.87 132.87 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 95.350 |
High resolution limit [Å] _reflns.d_resolution_high | 2.150 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.090 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 21347 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 91.5 |
Multiplicity _reflns.pdbx_redundancy | 4.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2VET |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2007-10-26 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 15.1 - 2.200 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1850 / 0.2050 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | PDB ENTRIES 1FFL AND 1FWM |