| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Australian Synchrotron |
Beamline _diffrn_source.pdbx_synchrotron_beamline | MX1 |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2014-06-30 |
Detector _diffrn_detector.type | ADSC QUANTUM 210r |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.9537 |
| Software | |
Data reduction _software.classification | iMOSFLM |
Data scaling _software.classification | SCALA |
Phasing _software.classification | PHASER |
Refinement _software.classification | PHENIX (1.10.1_2155: ???) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 67.590 79.010 95.821 87.64 73.29 89.97 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.95370 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 50.350 |
High resolution limit [Å] _reflns.d_resolution_high | 2.100 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.129 |
| Rmeas | - |
Rpim _reflns.pdbx_Rpim_I_all | 0.061 |
| Total number of observations | - |
Total number unique _reflns.number_obs | 106633 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 41.65 |
Completeness [%] _reflns.percent_possible_obs | 96.3 |
Multiplicity _reflns.pdbx_redundancy | 5.4 |
CC(1/2) _reflns.pdbx_CC_half | 0.995 |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 5V4M |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2017-03-10 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 48.3 - 2.100 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2167 / 0.2440 |