| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Photon Factory |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL-6A |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1992-03 |
Detector _diffrn_detector.type | WEISSENBERG |
| Software | |
Data reduction _software.classification | WEIS |
Refinement #1 _software.classification | TNT (5D) |
Refinement #2 _software.classification | TNT (V. 5-D) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 107.9 207.5 509.9 90.0 94.7 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 4V40 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1994-07-18 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 8.0 - 2.500 Å |
R _refine.ls_R_factor_obs | 0.1740 WARNING: neither Rwork nor Rfree given |