Data quality metrics extracted from 7uk0.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 7UK0 at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 19-ID
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
19-ID
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2022-03-25
Detector
_diffrn_detector.type
ADSC QUANTUM 315r
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.02466, 1.00743
Software
Data reduction
_software.classification
autoPROC
Data scaling
_software.classification
STARANISO
Phasing
_software.classification
AutoSol
Refinement
_software.classification
PHENIX (1.19.2_4158)
General information
Spacegroup name
_symmetry.space_group_name_H-M
H 3
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
106.855 106.855 88.652 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.024661.00743 Å

Data quality metricsOverallOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 64.020 4.940
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 4.360 4.360
  Rmerge - -
  Rmeas - -
  Rpim - -
  Total number of observations - -
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_obs
 3292 412
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 4.20 -
Completeness [%] 
_reflns.percent_possible_obs
 85.3 -
Multiplicity 
_reflns.pdbx_redundancy
 5.1 -
CC(1/2) 
_reflns.pdbx_CC_half _reflns_shell.pdbx_CC_half
 0.996 0.264

Refinement
PDB entry ID
_entry.id
7UK0
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2022-03-31
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
41.0 - 4.360 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2418 / 0.2750
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD