Data quality metrics extracted from 5ucb.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 5UCB at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
APS BEAMLINE 21-ID-D
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
21-ID-D
Temperature [K]
_diffrn.ambient_temp
193
Detector technology
_diffrn_detector.detector
PIXEL
Collection date
_diffrn_detector.pdbx_collection_date
2015-06-15
Detector
_diffrn_detector.type
DECTRIS PILATUS3 6M
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.033
Software
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
MOLREP
Refinement
_software.classification
PHENIX (1.11.1_2575: ???)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
45.378 49.180 84.707 106.29 95.71 100.13
Wavelength
_diffrn_radiation_wavelength.wavelength
1.03300 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 35.589
High resolution limit [Å] 
_reflns.d_resolution_high
 1.521
  Rmerge -
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 100518
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 32.20
Completeness [%] 
_reflns.percent_possible_obs
 95.8
Multiplicity 
_reflns.pdbx_redundancy
 3.2
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
5UCB
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2016-12-22
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
35.6 - 1.521 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1381 / 0.1688