Data quality metrics extracted from 1u9p.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1U9P at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
ROTATING ANODE
Source details
_diffrn_source.type
RIGAKU RU200
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
APS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
8-BM
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2003-08-16
Detector
_diffrn_detector.type
ADSC QUANTUM 315
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.541
Software
Data collection
_software.classification
HKL-2000
Data reduction
_software.classification
HKL-2000
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
CNS
Refinement
_software.classification
CNS
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 1 21 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
29.181 62.916 30.380 90.00 102.69 90.00
Wavelength
_diffrn_radiation_wavelength.wavelength
0.979001.54100 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 20.000
High resolution limit [Å] 
_reflns.d_resolution_high
 1.900
Rmerge 
_reflns.pdbx_Rsym_value
 0.067
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 8500
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 11.50
Completeness [%] 
_reflns.percent_possible_obs
 95.0
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1U9P
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2004-08-10
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
20.0 - 1.900 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.2490 / 0.2970
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD