| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Detector technology _diffrn_detector.detector | DIFFRACTOMETER |
Collection date _diffrn_detector.pdbx_collection_date | 1993-06-21 |
Detector _diffrn_detector.type | ENRAF-NONIUS FAST |
| Software | |
Data reduction #1 _software.classification | MADNES |
Data reduction #2 _software.classification | PROCOR |
Data reduction #3 _software.classification | FBSCALE |
Refinement _software.classification | GPRLSA |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 63 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 127.52 127.52 68.25 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 15.000 |
High resolution limit [Å] _reflns.d_resolution_high | 1.950 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.087 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 48550 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 98.0 |
Multiplicity _reflns.pdbx_redundancy | 3.6 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1TSD |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-08-15 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 7.0 - 1.950 Å |
R _refine.ls_R_factor_obs | 0.1970 WARNING: neither Rwork nor Rfree given |