| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | NSLS BEAMLINE X12C |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | NSLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X12C |
Detector technology _diffrn_detector.detector | IMAGE PLATE AREA DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 1994-03 |
Detector _diffrn_detector.type | MARRESEARCH |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 1.00,0.9802,0.9795,0.930 |
| Software | |
Data reduction _software.classification | MOSFLM |
Phasing _software.classification | X-PLOR |
Model building _software.classification | X-PLOR |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 72.5 30.2 43.4 90.00 100.11 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.000000.980200.979500.93000 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1TIG |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-08-16 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 6.0 - 2.000 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2070 / 0.2740 |