| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | NSLS BEAMLINE X8C |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | NSLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X8C |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 1992-10-24 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.98 |
| Software | |
Data collection #1 _software.classification | MADNES |
Data collection #2 _software.classification | PROCOR |
Data reduction #1 _software.classification | MADNES |
Data reduction #2 _software.classification | PROCOR |
Refinement _software.classification | PROLSQ |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 61 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 93.0 93.0 74.4 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.98000 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1TDR |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-04-13 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 16.0 - 2.500 Å |
R _refine.ls_R_factor_obs | 0.1240 WARNING: neither Rwork nor Rfree given |