Experiment | |
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Method _exptl.method | X-RAY DIFFRACTION The method used in the experiment. |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH SINGLE WAVELENGTH, LAUE, or MAD. |
Software | |
Data reduction _software.classification | DENZO The classification of the program according to its |
Data scaling _software.classification | SCALEPACK The classification of the program according to its |
Phasing _software.classification | X-PLOR The classification of the program according to its |
Refinement _software.classification | REFMAC (refmac_5.1.19; 24/04/2001; Murshudov, G.N.; ccp4@dl.ac.uk) The classification of the program according to its |
General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 2 Hermann-Mauguin space-group symbol. Note that the |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 255.26 Unit-cell length a corresponding to the structure reported in 265.25 Unit-cell length b corresponding to the structure reported in 184.40 Unit-cell length c corresponding to the structure reported in 90.0 Unit-cell angle alpha of the reported structure in degrees. 90.0 Unit-cell angle beta of the reported structure in degrees. 90.0 Unit-cell angle gamma of the reported structure in degrees. |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
Data quality metrics | Overall |
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Low resolution limit [Å] _reflns.d_resolution_low | 40.000 The largest value in angstroms for the interplanar spacings |
High resolution limit [Å] _reflns.d_resolution_high | 3.000 The smallest value in angstroms for the interplanar spacings |
Rmerge | - |
Rmeas | - |
Rpim | - |
Total number of observations | - |
Total number unique _reflns.number_obs | 241858 The number of reflections in the REFLN list (not the DIFFRN_REFLN |
<I/σ(I)> | - |
Completeness [%] | - |
Multiplicity | - |
CC(1/2) | - |
Refinement | |
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PDB entry ID _entry.id | 1SX4 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2004-03-30 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 40.0 - 3.000 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2575 / 0.2873 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | WARNING: no starting model (for MR) given |