| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | DIAMOND BEAMLINE I03 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Diamond |
Beamline _diffrn_source.pdbx_synchrotron_beamline | I03 |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | PIXEL |
Collection date _diffrn_detector.pdbx_collection_date | 2017-10-05 |
Detector _diffrn_detector.type | DECTRIS EIGER2 XE 16M |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.97629 |
| Software | |
Data reduction _software.classification | XDS |
Data scaling _software.classification | Aimless |
Phasing _software.classification | BUSTER |
Refinement _software.classification | REFMAC (5.8.0232) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 45.723 213.727 55.842 90.00 96.96 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.97629 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 106.860 |
High resolution limit [Å] _reflns.d_resolution_high | 1.940 |
| Rmerge | - |
Rmeas _reflns.pdbx_Rrim_I_all | 0.044 |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 78707 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 13.80 |
Completeness [%] _reflns.percent_possible_obs | 99.7 |
Multiplicity _reflns.pdbx_redundancy | 3.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 8S0S |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2024-02-14 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 55.4 - 1.940 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2149 / 0.2585 |
Structure solution method _refine.pdbx_method_to_determine_struct | FOURIER SYNTHESIS |