Data quality metrics extracted from 1s0p.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 1S0P at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
MPG/DESY, HAMBURG BEAMLINE BW6
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
MPG/DESY, HAMBURG
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BW6
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
2002-04-30
Detector
_diffrn_detector.type
RIGAKU
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.9760, 0.9176, 1.105
Software
Data reduction
_software.classification
DENZO
Data scaling
_software.classification
SCALEPACK
Phasing
_software.classification
CNS
Refinement
_software.classification
CNS
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
37.52 42.13 53.74 97.42 105.09 97.15
Wavelength
_diffrn_radiation_wavelength.wavelength
0.976000.917601.10500 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 1.800
High resolution limit [Å] 
_reflns.d_resolution_high
 1.400
  Rmerge -
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 20092
  <I/σ(I)> -
  Completeness [%] -
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
1S0P
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2004-01-01
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
1.8 - 1.400 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1800 / 0.2100
Structure solution method
_refine.pdbx_method_to_determine_struct
SIRAS