| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | CHESS BEAMLINE F1 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | CHESS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | F1 |
Temperature [K] _diffrn.ambient_temp | 258.00 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1993-09-01 |
Detector _diffrn_detector.type | FUJI |
| Software | |
Data collection _software.classification | PURDUE (SOFTWARE) |
Data reduction _software.classification | PURDUE (DATA PROCESSING PACKAGE) |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 2 2 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 137.29 153.10 76.20 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 40.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.700 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.106 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 18147 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 83.7 |
Multiplicity _reflns.pdbx_redundancy | 4.6 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1RUO |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-05-26 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.700 Å |
Rwork _refine.ls_R_factor_R_work | 0.2130 WARNING: no Rfree given (but Rwork)!? |