| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SRS BEAMLINE PX9.6 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SRS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | PX9.6 |
Detector technology _diffrn_detector.detector | FILM |
Collection date _diffrn_detector.pdbx_collection_date | 1988-06 |
Detector _diffrn_detector.type | KODAK |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.895 |
| Software | |
Data reduction _software.classification | PURDUE (DATA PROCESSING PACKAGE) |
Model building _software.classification | O |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 3 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 445.1 445.1 445.1 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.89500 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 30.000 |
High resolution limit [Å] _reflns.d_resolution_high | 3.000 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.147 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 19125 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 4.0 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1RUJ |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-06-09 |