| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | PHOTON FACTORY |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Photon Factory |
Temperature [K] _diffrn.ambient_temp | 284 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1990-05-22 |
Detector _diffrn_detector.type | FUJI |
| Software | |
Data collection _software.classification | OSCMGR (LOCAL VERSION) |
Data reduction #1 _software.classification | TOMOKO |
Data reduction #2 _software.classification | MARIKO (LOCAL PROGRAM) |
Data reduction #3 _software.classification | OSC (LOCAL VERSION) |
Data scaling #1 _software.classification | A (PROGRAM BY TOMOKO) |
Data scaling #2 _software.classification | MARIKO |
Phasing _software.classification | X-PLOR |
Model building _software.classification | X-PLOR |
Refinement #1 _software.classification | PROLSQ |
Refinement #2 _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 49.32 61.27 34.95 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.90000 Å |
| Data quality metrics | Overall | OuterShell |
|---|---|---|
Low resolution limit [Å] _reflns.d_resolution_low _reflns_shell.d_res_low | 12.000 | 1.870 |
High resolution limit [Å] _reflns.d_resolution_high _reflns_shell.d_res_high | 1.800 | 1.800 |
Rmerge _reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs | 0.034 | 0.077 |
| Rmeas | - | - |
| Rpim | - | - |
| Total number of observations | - | - |
Total number unique _reflns.number_obs | 9903 | - |
| <I/σ(I)> | - | - |
Completeness [%] _reflns.percent_possible_obs _reflns_shell.percent_possible_all | 96.1 | 86.4 |
Multiplicity _reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy | 4.0 | 3.0 |
| CC(1/2) | - | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1RTU |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1995-05-12 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 8.0 - 1.800 Å |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | RNASE T1 (PDB ENTRY 1RNT) |