| Experiment | |
|---|---|
Method _exptl.method | FIBER DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | ELLIOT GX-6 |
Temperature [K] _diffrn.ambient_temp | 298 |
Detector technology _diffrn_detector.detector | FILM |
Collection date _diffrn_detector.pdbx_collection_date | 1990-10 |
Detector _diffrn_detector.type | KODAK FILM |
| Software | |
Data reduction _software.classification | RADPV |
Data scaling _software.classification | SCALV |
Refinement _software.classification | FXPLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 1.0 1.0 1.0 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 50.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.800 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 6045 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 91.2 |
Multiplicity _reflns.pdbx_redundancy | 4.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1RMV |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-02-11 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.900 Å |
Rwork _refine.ls_R_factor_R_work | 0.0950 WARNING: no Rfree given (but Rwork)!? |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | PDB ENTRY 2TMV |