Experiment | |
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Method _exptl.method | X-RAY DIFFRACTION The method used in the experiment. |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH SINGLE WAVELENGTH, LAUE, or MAD. |
Source type _diffrn_source.source | SYNCHROTRON The general class of the radiation source. |
Source details _diffrn_source.type | ESRF BEAMLINE ID14-1 The make, model or name of the source of radiation. |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | ESRF Synchrotron site. |
Beamline _diffrn_source.pdbx_synchrotron_beamline | ID14-1 Synchrotron beamline. |
Temperature [K] _diffrn.ambient_temp | 100 The mean temperature in kelvins at which the intensities were |
Detector technology _diffrn_detector.detector | CCD The general class of the radiation detector. |
Collection date _diffrn_detector.pdbx_collection_date | 2006-11-17 The date of data collection. |
Detector _diffrn_detector.type | ADSC QUANTUM 210 The make, model or name of the detector device used. |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.9330 Comma separated list of wavelengths or wavelength range. |
Software | |
Data collection _software.classification | MxCuBE The classification of the program according to its |
Data reduction _software.classification | MOSFLM (A.G.W. Leslie; andrew@mrc-lmb.cam.ac.uk) The classification of the program according to its |
Data scaling _software.classification | SCALA (Phil Evans; pre@mrc-lmb.cam.ac.uk) The classification of the program according to its |
Phasing #1 _software.classification | SHARP (de La Fortelle; sharp-develop@globalphasing.com) The classification of the program according to its |
Phasing #2 _software.classification | SOLOMON (Abrahams J. P.; ccp4@dl.ac.uk) The classification of the program according to its |
Refinement _software.classification | REFMAC (refmac_5.2.0019; 24/04/2001; Murshudov, G.N.; ccp4@dl.ac.uk) The classification of the program according to its |
General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 Hermann-Mauguin space-group symbol. Note that the |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 28.655 Unit-cell length a corresponding to the structure reported in 48.217 Unit-cell length b corresponding to the structure reported in 54.406 Unit-cell length c corresponding to the structure reported in 90.0 Unit-cell angle alpha of the reported structure in degrees. 90.0 Unit-cell angle beta of the reported structure in degrees. 90.0 Unit-cell angle gamma of the reported structure in degrees. |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.28230 The radiation wavelength in angstroms. 1.28310 The radiation wavelength in angstroms. 1.27700 The radiation wavelength in angstroms. 0.93300 ÅThe radiation wavelength in angstroms. |
Refinement | |
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PDB entry ID _entry.id | 2RKN |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2007-10-17 |