Data quality metrics extracted from 2rfm.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 2RFM at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
ROTATING ANODE
Source details
_diffrn_source.type
RIGAKU
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
BESSY
Beamline
_diffrn_source.pdbx_synchrotron_beamline
14.2
Temperature [K]
_diffrn.ambient_temp
180
Detector technology
_diffrn_detector.detector
IMAGE PLATE
Collection date
_diffrn_detector.pdbx_collection_date
2006-02-12
Detector
_diffrn_detector.type
RIGAKU
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.5418
Software
Data collection
_software.classification
CrystalClear
Data reduction
_software.classification
MOSFLM
Data scaling
_software.classification
SCALA (Phil Evans; pre@mrc-lmb.cam.ac.uk)
Phasing #1
_software.classification
SHELX (George Sheldrick; gsheldr@shelx.uni-ac.gwdg.de)
Phasing #2
_software.classification
SHELXD
Refinement
_software.classification
REFMAC (Murshudov, G.N.; ccp4@dl.ac.uk)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 64 2 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
101.002 101.002 174.483 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.923801.54180 Å

Data quality metricsOverallInnerShellOuterShell
Low resolution limit [Å] 
_reflns.d_resolution_low _reflns_shell.d_res_low
 48.472 61.660 1.740
High resolution limit [Å] 
_reflns.d_resolution_high _reflns_shell.d_res_high
 1.650 5.220 1.650
Rmerge 
_reflns.pdbx_Rmerge_I_obs _reflns_shell.Rmerge_I_obs
 0.055 0.027 0.323
  Rmeas - - -
  Rpim - - -
Total number of observations 
_reflns_shell.number_measured_all
 - 22182 37424
Total number unique 
_reflns.number_obs _reflns_shell.number_unique_all
 58965 2270 6052
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI _reflns_shell.meanI_over_sigI_obs
 7.20 19.90 2.40
Completeness [%] 
_reflns.percent_possible_obs _reflns_shell.percent_possible_all
 93.0 99.5 66.9
Multiplicity 
_reflns.pdbx_redundancy _reflns_shell.pdbx_redundancy
 9.9 9.8 6.2
  CC(1/2) - - -

Refinement
PDB entry ID
_entry.id
2RFM
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2007-10-01
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
20.0 - 1.650 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1560 / 0.1780
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD