Experiment | |
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Method _exptl.method | X-RAY DIFFRACTION The method used in the experiment. |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH SINGLE WAVELENGTH, LAUE, or MAD. |
Source type _diffrn_source.source | SYNCHROTRON The general class of the radiation source. |
Source details _diffrn_source.type | SSRL BEAMLINE BL9-2 The make, model or name of the source of radiation. |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SSRL Synchrotron site. |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL9-2 Synchrotron beamline. |
Detector technology _diffrn_detector.detector | CCD The general class of the radiation detector. |
Detector _diffrn_detector.type | MARMOSAIC 325 mm CCD The make, model or name of the detector device used. |
Software | |
Data reduction _software.classification | DENZO (Zbyszek Otwinowski; hkl@hkl-xray.com) The classification of the program according to its |
Data scaling _software.classification | SCALA (Phil R. Evans; pre@mrc-lmb.cam.ac.uk) The classification of the program according to its |
Phasing #1 _software.classification | PHASER (2.1.4; Fri Nov 14 10:05:38 2008; Randy J. Read; cimr-phaser@lists.cam.ac.uk) The classification of the program according to its |
Phasing #2 _software.classification | MOLREP The classification of the program according to its |
Refinement _software.classification | PHENIX (1.6.4_486; Paul D. Adams; PDAdams@lbl.gov) The classification of the program according to its |
General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 2 2 21 Hermann-Mauguin space-group symbol. Note that the |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 83.785 Unit-cell length a corresponding to the structure reported in 154.834 Unit-cell length b corresponding to the structure reported in 77.799 Unit-cell length c corresponding to the structure reported in 90.0 Unit-cell angle alpha of the reported structure in degrees. 90.0 Unit-cell angle beta of the reported structure in degrees. 90.0 Unit-cell angle gamma of the reported structure in degrees. |
Wavelength _diffrn_radiation_wavelength.wavelength | NA |
Data quality metrics | Overall |
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Low resolution limit [Å] _reflns.d_resolution_low | 28.500 The largest value in angstroms for the interplanar spacings |
High resolution limit [Å] _reflns.d_resolution_high | 1.790 The smallest value in angstroms for the interplanar spacings |
Rmerge _reflns.pdbx_Rsym_value | 0.059 The R sym value as a decimal number. |
Rmeas | - |
Rpim | - |
Total number of observations | - |
Total number unique _reflns.number_obs | 46701 The number of reflections in the REFLN list (not the DIFFRN_REFLN |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 17.50 The mean of the ratio of the intensities to their |
Completeness [%] _reflns.percent_possible_obs | 98.2 The percentage of geometrically possible reflections represented |
Multiplicity _reflns.pdbx_redundancy | 3.4 Overall redundancy for this data set. |
CC(1/2) | - |
Refinement | |
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PDB entry ID _entry.id | 3QPG |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2011-02-13 |