| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SLS BEAMLINE X10SA |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SLS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | X10SA |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2006-08-25 |
Detector _diffrn_detector.type | MARMOSAIC 225 mm CCD |
| Software | |
Data scaling _software.classification | XSCALE |
Phasing _software.classification | CNX |
Refinement #1 _software.classification | PHENIX (1.12_2829) |
Refinement #2 _software.classification | CNX |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 81.752 103.186 100.144 90.00 104.44 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.97945 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 58.239 |
High resolution limit [Å] _reflns.d_resolution_high | 2.120 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.048 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 91075 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 99.8 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 5QD7 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2017-12-01 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 58.2 - 2.120 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1650 / 0.1880 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | WARNING: no starting model (for MR) given |