Data quality metrics extracted from 3q3q.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 3Q3Q at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
MAD
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
ESRF BEAMLINE BM30A
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
ESRF
Beamline
_diffrn_source.pdbx_synchrotron_beamline
BM30A
Detector technology
_diffrn_detector.detector
CCD
Collection date
_diffrn_detector.pdbx_collection_date
2009-03-17
Detector
_diffrn_detector.type
ADSC QUANTUM 315r
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
0.976261, 0.980159, 0.980337
Software
Refinement
_software.classification
PHENIX (1.5_2; Paul D. Adams; PDAdams@lbl.gov)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 41 21 2
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
87.37 87.37 168.16 90.0 90.0 90.0
Wavelength
_diffrn_radiation_wavelength.wavelength
0.980160.976260.98034 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 49.785
High resolution limit [Å] 
_reflns.d_resolution_high
 1.950
  Rmerge -
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 87058
  <I/σ(I)> -
  Completeness [%] -
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
3Q3Q
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2010-12-22
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
49.8 - 1.953 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1553 / 0.1863
Structure solution method
_refine.pdbx_method_to_determine_struct
MAD