| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | ELLIOTT GX-13 |
Temperature [K] _diffrn.ambient_temp | 261 |
Collection date _diffrn_detector.pdbx_collection_date | 1995 |
| Software | |
Phasing _software.classification | X-PLOR |
Model building _software.classification | X-PLOR |
Refinement _software.classification | X-PLOR |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 322.94 358.04 380.15 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 999.900 |
High resolution limit [Å] _reflns.d_resolution_high | 2.900 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.148 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 306408 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 24.0 |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1PO2 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-01-08 |
Rwork _refine.ls_R_factor_R_work | 0.2490 WARNING: no Rfree given (but Rwork)!? |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | REFINED STRUCTURE OF P1/MAHONEY (2PLV), AFTER OMITTING ALL LIGANDS, SOLVENT, AND ANY AMINO ACID LOCATED CLOSE TO A SIGNIFICANT ELECTRON DENSITY FEATURE IN THE NON-CRYSTALLOGRAPHIC SYMMETRY-AVERAGED DIFFERENCE MAP. |