| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Collection date _diffrn_detector.pdbx_collection_date | 1989-01-01 |
Detector _diffrn_detector.type | CRAD, P21 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 1.5418 |
| Software | |
Data collection _software.classification | DTP (MIT) |
Data reduction _software.classification | DTP |
Refinement _software.classification | PROLSQ |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | I 4 2 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 53.59 53.59 69.79 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 10.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.500 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.123 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 2106 |
| <I/σ(I)> | - |
Completeness [%] _reflns.percent_possible_obs | 61.5 |
Multiplicity _reflns.pdbx_redundancy | 2.0 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2PLH |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1993-07-09 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 10.0 - 2.500 Å |
R _refine.ls_R_factor_obs | 0.1550 WARNING: neither Rwork nor Rfree given |