| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | ROTATING ANODE |
Source details _diffrn_source.type | RIGAKU RUH2R |
Temperature [K] _diffrn.ambient_temp | 293 |
Detector technology _diffrn_detector.detector | AREA DETECTOR |
Collection date _diffrn_detector.pdbx_collection_date | 1994-04-10 |
Detector _diffrn_detector.type | SIEMENS |
| Software | |
Data reduction _software.classification | XENGEN |
Data scaling _software.classification | XENGEN |
Refinement _software.classification | PROLSQ |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | I 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 196.32 127.12 134.13 90.0 97.6 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.54180 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 15.000 |
High resolution limit [Å] _reflns.d_resolution_high | 1.960 |
Rmerge _reflns.pdbx_Rsym_value | 0.100 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 189802 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 8.17 |
Completeness [%] _reflns.percent_possible_obs | 81.4 |
Multiplicity _reflns.pdbx_redundancy | 2.2 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 3PCG |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1997-04-29 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 6.0 - 1.960 Å |
Rwork _refine.ls_R_factor_R_work | 0.1750 WARNING: no Rfree given (but Rwork)!? |
Structure solution method _refine.pdbx_method_to_determine_struct | NATIVE MODEL PHASES |