| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | PHOTON FACTORY BEAMLINE BL-6A |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | Photon Factory |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL-6A |
Temperature [K] _diffrn.ambient_temp | 283 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 1996-05-19 |
Detector _diffrn_detector.type | FUJI |
| Software | |
Data reduction #1 _software.classification | DENZO |
Data reduction #2 _software.classification | TSUKI (SCALE (LOCAL)) |
Data scaling #1 _software.classification | SCALEPACK |
Data scaling #2 _software.classification | TSUKI (SCALE (LOCAL)) |
Phasing _software.classification | X-PLOR (3.84) |
Model building _software.classification | X-PLOR (3.84) |
Refinement _software.classification | X-PLOR (3.84) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 21 21 21 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 189.1 210.5 178.6 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.00000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 100.000 |
High resolution limit [Å] _reflns.d_resolution_high | 2.350 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.062 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 270061 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 14.40 |
Completeness [%] _reflns.percent_possible_obs | 89.2 |
Multiplicity _reflns.pdbx_redundancy | 4.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1OCR |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1998-07-07 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 15.0 - 2.350 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2030 / 0.2470 |
Structure solution method _refine.pdbx_method_to_determine_struct | MULTIPLE ISOMORPHOUS REPLACEMENT |