| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | OTHER |
Temperature [K] _diffrn.ambient_temp | 297 |
Detector technology _diffrn_detector.detector | FILM |
Collection date _diffrn_detector.pdbx_collection_date | 1987 |
Detector _diffrn_detector.type | FILM |
| Software | |
Data reduction _software.classification | MOSFLM |
Phasing _software.classification | BLANC |
Model building _software.classification | BLANC |
Refinement _software.classification | PROLSQ |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 63 2 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 159.42 159.42 106.86 90.0 90.0 120.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.50000 Å |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1OBR |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 1996-06-22 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 7.0 - 2.300 Å |
Rwork _refine.ls_R_factor_R_work | 0.1520 WARNING: no Rfree given (but Rwork)!? |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | CARBOXYPEPTIDASE A (PDB ENTRY 5CPA) |