Data quality metrics extracted from 4o9x.cif.gz by aB_cif2table1 from BUSTER (Global Phasing Ltd.). See also the PDBx/mmCIF dictionary and a MXLIMS-compatible JSON representation.

Experimental information for 4O9X at RCSB, PDBe, PDBj

Experiment
Method
_exptl.method
X-RAY DIFFRACTION
Experimental protocol
_diffrn_radiation.pdbx_diffrn_protocol
SINGLE WAVELENGTH
Source type
_diffrn_source.source
SYNCHROTRON
Source details
_diffrn_source.type
SLS BEAMLINE X10SA
Synchrotron site
_diffrn_source.pdbx_synchrotron_site
SLS
Beamline
_diffrn_source.pdbx_synchrotron_beamline
X10SA
Temperature [K]
_diffrn.ambient_temp
100
Detector technology
_diffrn_detector.detector
PIXEL
Collection date
_diffrn_detector.pdbx_collection_date
2012-09-20
Detector
_diffrn_detector.type
DECTRIS PILATUS 6M
Wavelength(s) [Å]
_diffrn_source.pdbx_wavelength_list
1.07169
Software
Data reduction
_software.classification
XDS
Data scaling #1
_software.classification
XSCALE (Wolfgang Kabsch)
Data scaling #2
_software.classification
XDS
Phasing
_software.classification
PHENIX
Refinement
_software.classification
PHENIX (1.8.1_1168; Paul D. Adams; PDAdams@lbl.gov)
General information
Spacegroup name
_symmetry.space_group_name_H-M
P 32 2 1
Unit cell parameters
_cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma}
232.36 232.36 143.57 90.0 90.0 120.0
Wavelength
_diffrn_radiation_wavelength.wavelength
1.007171.07169 Å

Data quality metricsOverall
Low resolution limit [Å] 
_reflns.d_resolution_low
 30.000
High resolution limit [Å] 
_reflns.d_resolution_high
 2.170
Rmerge 
_reflns.pdbx_Rmerge_I_obs
 0.178
  Rmeas -
  Rpim -
  Total number of observations -
Total number unique 
_reflns.number_obs
 183387
<I/σ(I)> 
_reflns.pdbx_netI_over_sigmaI
 17.47
Completeness [%] 
_reflns.percent_possible_obs
 99.3
  Multiplicity -
  CC(1/2) -

Refinement
PDB entry ID
_entry.id
4O9X
Deposition date
_pdbx_database_status.recvd_initial_deposition_date
2014-01-03
Resolution
_refine.ls_d_res_low _refine.ls_d_res_high
29.8 - 2.170 Å
Rwork/Rfree
_refine.ls_R_factor_R_work _refine.ls_R_factor_R_free
0.1922 / 0.2155
Structure solution method
_refine.pdbx_method_to_determine_struct
SAD