| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | ALS BEAMLINE 8.2.2 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | ALS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | 8.2.2 |
Temperature [K] _diffrn.ambient_temp | 105 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2005-12-05 |
Detector _diffrn_detector.type | ADSC QUANTUM 315 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.97965, 0.97983, 0.96441 |
| Software | |
Data collection _software.classification | ADSC (QUANTUM) |
Data reduction _software.classification | MOSFLM |
Data scaling _software.classification | CCP4 (SCALA) |
Phasing _software.classification | SHELXS |
Refinement _software.classification | REFMAC (5.2.0019) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 255.130 142.769 62.025 90.00 99.49 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.979650.979830.964411.07210 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 62.900 |
High resolution limit [Å] _reflns.d_resolution_high | 1.940 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.067 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 147021 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 14.80 |
Completeness [%] _reflns.percent_possible_obs | 91.1 |
Multiplicity _reflns.pdbx_redundancy | 4.4 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 2O4V |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2006-12-05 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 62.9 - 1.940 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1743 / 0.1940 |
Structure solution method _refine.pdbx_method_to_determine_struct | MAD |