| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SSRL BEAMLINE BL7-1 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SSRL |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL7-1 |
Detector technology _diffrn_detector.detector | CCD |
Collection date _diffrn_detector.pdbx_collection_date | 2012-06-26 |
Detector _diffrn_detector.type | ADSC QUANTUM 315r |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 1.2836 |
| Software | |
Data reduction _software.classification | HKL-2000 |
Data scaling #1 _software.classification | XDS |
Data scaling #2 _software.classification | HKL-2000 |
Phasing _software.classification | PHASER |
Refinement _software.classification | PHENIX (1.7.2_869; Paul D. Adams; PDAdams@lbl.gov) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | C 1 2 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 202.93 52.18 75.82 90.00 105.21 90.00 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.28360 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 48.955 |
High resolution limit [Å] _reflns.d_resolution_high | 3.020 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.083 |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 13566 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 17.00 |
Completeness [%] _reflns.percent_possible_obs | 98.7 |
Multiplicity _reflns.pdbx_redundancy | 4.1 |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 4N2C |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2013-10-04 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 49.0 - 3.022 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.2453 / 0.2728 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | PDB ENTRY 4N25 |