| Experiment | |
|---|---|
Method _exptl.method | ELECTRON CRYSTALLOGRAPHY |
Collection date _diffrn_detector.pdbx_collection_date | 2018-10-03 |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.0251 |
| Software | |
Data reduction _software.classification | MOSFLM (7.2.2) |
Data scaling _software.classification | Aimless (0.7.3) |
Phasing _software.classification | MOLREP (11.6.04) |
Refinement _software.classification | REFMAC (5.8.0238) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 43 21 2 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 26.219 26.219 27.534 90.0 90.0 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.02510 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 18.990 |
High resolution limit [Å] _reflns.d_resolution_high | 1.900 |
Rmerge _reflns.pdbx_Rmerge_I_obs | 0.236 |
Rmeas _reflns.pdbx_Rrim_I_all | 0.251 |
Rpim _reflns.pdbx_Rpim_I_all | 0.084 |
| Total number of observations | - |
Total number unique _reflns.number_obs | 686 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 5.10 |
Completeness [%] _reflns.percent_possible_obs | 78.6 |
Multiplicity _reflns.pdbx_redundancy | 8.1 |
CC(1/2) _reflns.pdbx_CC_half | 0.985 |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 6MXF |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2018-10-30 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 19.0 - 1.910 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1905 / 0.2180 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | 1e9w |