| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | APS BEAMLINE 24-ID-C |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | APS |
Beamline _diffrn_source.pdbx_synchrotron_beamline | 24-ID-C |
Temperature [K] _diffrn.ambient_temp | 100 |
Detector technology _diffrn_detector.detector | PIXEL |
Collection date _diffrn_detector.pdbx_collection_date | 2019-07-28 |
Detector _diffrn_detector.type | DECTRIS EIGER2 X 16M |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 1.8917 |
| Software | |
Data reduction _software.classification | XDS |
Data scaling #1 _software.classification | Aimless |
Data scaling #2 _software.classification | pointless |
Phasing _software.classification | PHENIX |
Refinement _software.classification | PHENIX (1.17_3644) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 71.681 127.799 128.809 90.000 94.872 90.000 |
Wavelength _diffrn_radiation_wavelength.wavelength | 1.89170 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 128.340 |
High resolution limit [Å] _reflns.d_resolution_high | 2.350 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 174471 |
<I/σ(I)> _reflns.pdbx_netI_over_sigmaI | 11.00 |
Completeness [%] _reflns.percent_possible_obs | 98.8 |
Multiplicity _reflns.pdbx_redundancy | 6.6 |
CC(1/2) _reflns.pdbx_CC_half | 0.994 |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 7MPQ |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2021-05-04 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 128.3 - 2.350 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1619 / 0.2063 |
Structure solution method _refine.pdbx_method_to_determine_struct | MOLECULAR REPLACEMENT |
Starting model (for MR) _refine.pdbx_starting_model | 1yt3 |