| Experiment | |
|---|---|
Method _exptl.method | X-RAY DIFFRACTION |
Experimental protocol _diffrn_radiation.pdbx_diffrn_protocol | SINGLE WAVELENGTH |
Source type _diffrn_source.source | SYNCHROTRON |
Source details _diffrn_source.type | SSRL BEAMLINE BL9-1 |
Synchrotron site _diffrn_source.pdbx_synchrotron_site | SSRL |
Beamline _diffrn_source.pdbx_synchrotron_beamline | BL9-1 |
Temperature [K] _diffrn.ambient_temp | 93 |
Detector technology _diffrn_detector.detector | IMAGE PLATE |
Collection date _diffrn_detector.pdbx_collection_date | 2000-02-19 |
Detector _diffrn_detector.type | MAR scanner 345 mm plate |
Wavelength(s) [Å] _diffrn_source.pdbx_wavelength_list | 0.78 |
| Software | |
Data collection _software.classification | Blu-Ice |
Data reduction #1 _software.classification | MOSFLM |
Data reduction #2 _software.classification | DENZO |
Data scaling #1 _software.classification | SCALEPACK |
Data scaling #2 _software.classification | SCALA |
Data scaling #3 _software.classification | CCP4 (SCALA) |
Phasing #1 _software.classification | SOLVE |
Phasing #2 _software.classification | DM |
Model building #1 _software.classification | DM |
Model building #2 _software.classification | WARP |
Model building #3 _software.classification | ARP/wARP |
Refinement _software.classification | CNS (1.0) |
| General information | |
Spacegroup name _symmetry.space_group_name_H-M | P 1 21 1 |
Unit cell parameters _cell.length_{a,b,c} _cell.angle_{alpha,beta,gamma} | 87.98 60.12 105.60 90.0 102.5 90.0 |
Wavelength _diffrn_radiation_wavelength.wavelength | 0.78000 Å |
| Data quality metrics | Overall |
|---|---|
Low resolution limit [Å] _reflns.d_resolution_low | 20.000 |
High resolution limit [Å] _reflns.d_resolution_high | 1.650 |
| Rmerge | - |
| Rmeas | - |
| Rpim | - |
| Total number of observations | - |
Total number unique _reflns.number_obs | 129754 |
| <I/σ(I)> | - |
| Completeness [%] | - |
| Multiplicity | - |
| CC(1/2) | - |
| Refinement | |
|---|---|
PDB entry ID _entry.id | 1MO9 |
Deposition date _pdbx_database_status.recvd_initial_deposition_date | 2002-09-08 |
Resolution _refine.ls_d_res_low _refine.ls_d_res_high | 19.9 - 1.650 Å |
Rwork/Rfree _refine.ls_R_factor_R_work _refine.ls_R_factor_R_free | 0.1880 / 0.2130 |
Structure solution method _refine.pdbx_method_to_determine_struct | MIRAS |